@article{Kusch2018, author = {Peter Kusch}, title = {Headspace Solid-Phase Microextraction Coupled with Gas Chromatography–Mass Spectrometry for the Characterization of Polymeric Materials}, series = {LC-GC North America}, volume = {36}, number = {1}, publisher = {Advanstar Communications}, issn = {0888-9090}, pages = {52 -- 61}, year = {2018}, abstract = {For the last 20 years, solid-phase microextraction (SPME) in headspace (HS) mode has been used as a valuable sample preparation technique for identifying degradation products in polymers and the determination of residual monomers and other light-boiling substances in polymeric materials. For more than 10 years, our laboratory has been involved in projects focused on the application of HS-SPME-gas chromatography–mass spectrometry (GC–MS) for the characterization of polymeric materials from many branches of manufacturing and building industries. This article describes the application of this technique for identifying volatile organic compounds (VOCs), additives, and degradation products in industrial rubber, car labeling reflection foil, and bone cement materials. The obtained analytical results were then used for troubleshooting and remedial action of the technological processes as well as for the health protection of producers and users.}, language = {en} }