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Development of an Advanced Dynamic Microindentation System to Determine Local Viscoelastic Properties of Polymers

  • This study presents a microindentation system which allows spatially resolved local as well as bulk viscoelastic material information to be obtained within one instrument. The microindentation method was merged with dynamic mechanical analysis (DMA) for a tungsten cone indenter. Three tungsten cone indenters were investigated: tungsten electrode, tungsten electrode + 2% lanthanum, and tungsten electrode + rare earth elements. Only the tungsten electrode + 2% lanthanum indenter showed the sinusoidal response, and its geometry remained unaffected by the repeated indentations. Complex moduli obtained from dynamic microindentation for high-density polyethylene, polybutylene terephthalate, polycarbonate, and thermoplastic polyurethane are in agreement with the literature. Additionally, by implementing a specially developed x-y-stage, this study showed that dynamic microindentation with a tungsten cone indenter was an adequate method to determine spatially resolved local viscoelastic surface properties.

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Metadaten
Document Type:Article
Language:German
Volume:11
Issue:5
First Page:833
URN:urn:nbn:de:hbz:1044-opus-44919
DOI:https://doi.org/10.3390/polym11050833
Pubmed Id:http://www.ncbi.nlm.nih.gov/pubmed?term=31071983
Publisher:MDPI
Place of publication:Basel
Date of first publication:2019/05/25
Departments, institutes and facilities:Fachbereich Angewandte Naturwissenschaften
Dewey Decimal Classification (DDC):5 Naturwissenschaften und Mathematik / 54 Chemie / 540 Chemie und zugeordnete Wissenschaften
Entry in this database:2019/05/25
Licence (German):License LogoCreative Commons - CC BY - Namensnennung 4.0 International